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HRID514707

反应详情

EQUATION

反应方程式

HRID 514707 的结构方程式

REACTANTS

反应物

1
结构：O=[N+]([O-])c1cccc(CS(=O)(=O)C2CC2)c1
HCID70976459

未命名化合物

PRODUCTS

生成物

1
结构：Nc1cccc(CS(=O)(=O)C2CC2)c1
HCID86729613

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：[Cl-].[Cl-].[Cl-].[Ti+3]
催化剂HCID10313229

未命名化合物

结构：Cl
溶剂HCID313

Hydrochloric Acid

ClH

PROCEDURE

实验过程

was prepared under similar conditions as described in the preparation of Intermediate 1.3. using 1-[(cyclopropylsulfonyl)methyl]-3-nitrobenzene and titanium(III)chloride solution (about 15%) in about 10% hydrochloric acid (Merck Schuchardt OHG). The batch was purified by chromatography (DCM/EtOH 95:5).

WORKUP

后处理

  1. customwas prepared under similar conditions
  2. customThe batch was purified by chromatography (DCM/EtOH 95:5)