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HRID522131

反应详情

EQUATION

反应方程式

HRID 522131 的结构方程式

REACTANTS

反应物

2
结构：O=C(O)c1cc(Br)ccc1Cl
HCID33127

5-Bromo-2-chlorobenzoic acid

C7H4BrClO2

结构：CCOC(=O)c1cc(N)n(-c2cccc(OCc3ccccc3)c2)n1
HCID118497040

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)c1cc(NC(=O)c2cc(Br)ccc2Cl)n(-c2cccc(OCc3ccccc3)c2)n1
HCID118497151

未命名化合物

PROCEDURE

实验过程

The title compound was prepared according to the method described for Preparation 16 using ethyl 5-amino-1-(3-(benzyloxy)phenyl)-1H-pyrazole-3-carboxylate (Preparation 54) and 2-chloro-5-bromobenzoic acid. The residue was purified using silica gel column chromatography eluting with 30-40% EtOAc in heptanes.

WORKUP

后处理

  1. customThe residue was purified
  2. washeluting with 30-40% EtOAc in heptanes