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HRID524616

反应详情

EQUATION

反应方程式

HRID 524616 的结构方程式

REACTANTS

反应物

2
结构：B
HCID6331

Borane

H3B

结构：CC1(C)OCC(=O)N(Cc2ccccc2)[C@@H]1C(=O)OCc1ccccc1
HCID118118261

未命名化合物

PRODUCTS

生成物

1
结构：CC1(C)OCCN(Cc2ccccc2)[C@@H]1C(=O)OCc1ccccc1
HCID118118262

未命名化合物

收率 85%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

(S)-benzyl 4-benzyl-2,2-dimethyl-5-oxomorpholine-3-carboxylate (163 g, 461 mmol) was reacted with a solution of borane in THF (1 mol/L, 692 mL) according to the procedure as described in Example 34, Step B to give the title compound as colorless oil (133 g, 85%). The compound was characterized by the following spectroscopic data: