huagongshe.com
HRID52593

反应详情

EQUATION

反应方程式

HRID 52593 的结构方程式

REACTANTS

反应物

3
结构：O=C1NC(=O)C(c2ccccc2)(c2ccccc2)N1
HCID1775

5,5-Diphenylhydantoin

C15H12N2O2

结构：N#Cc1cccc(CBr)c1
HCID97249

Benzonitrile, 3-(bromomethyl)-

C8H6BrN

结构：CC(C)(C)[O-].[K+]
HCID23665647

2-Methyl-2-propanol, potassium salt

C4H9KO

PRODUCTS

生成物

1
结构：N#Cc1cccc(CN2C(=O)NC(c3ccccc3)(c3ccccc3)C2=O)c1
HCID18975921

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

Prepared by reacting 25.5 g (0.101 Mol) of 5,5-diphenylhydantoin with 21.15 g (0.108 Mol) of 3-(bromomethyl)-benzonitrile in the presence of 12.0 g (0.107 Mol) of potassium tert.-butoxide and 200 ml of anhydrous dimethylformamide. After conventional working up 34.0 g (92% of theory) of colourless crystals were obtained, mp. 160°-164° C.

WORKUP

后处理

  1. customPrepared
  2. customwere obtained