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HRID53072

反应详情

EQUATION

反应方程式

HRID 53072 的结构方程式

REACTANTS

反应物

4
结构：Cl
HCID313

Hydrochloric Acid

ClH

2 次

结构：O=C(O)CCC(=O)O
HCID1110

Butanedioic acid

C4H6O4

结构：O=C([O-])CCC(=O)[O-].[Na+].[Na+]
HCID9020

Disodium succinate

C4H4Na2O4

结构：NCCCC[C@H](N)C(=O)O.O
HCID16211825

Lysine monohydrate

C6H16N2O3

PRODUCTS

生成物

1
结构：Cl.NCCCC[C@H](N)C(=O)O.NCCCC[C@H](N)C(=O)O.O=C([O-])CCC(=O)[O-].[Na+].[Na+]
HCID86749085

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

12 grams of L-lysine monohydrate is dissolved in 20 ml of water to which 6.0 ml of concentrated hydrochloric acid has been added. 2.964 grams of disodium succinate is added to neutralize some of the excess hydrochloric acid and 2.16 grams of succinic acid are added with mixing until effervescence ceases and all solids are dissolved. The solution is dried in a 110° C. oven until solids begin to form when cooled to room temperature. After 15 to 30 minutes solids form and are collected.

WORKUP

后处理

  1. additionhas been added
  2. additionare added
  3. additionwith mixing until effervescence ceases
  4. dissolutionall solids are dissolved
  5. customThe solution is dried in a 110° C. oven until solids
  6. customto form when
  7. customare collected