反应详情

2-Methylpentane-2,4-diol (2.8 ml) was dissolved in THF (20.0 ml) and NaH (60% in mineral oil; 1 g) was added. At room temperature 2,4-difluoronitrobenzene was added and the reaction mixture was stirred overnight. Then the reaction was quenched with water and concentrated in vacuo. The residue was dissolved in dichloromethane, washed with water and concentrated in vacuo.

1. customThen the reaction was quenched with water
2. concentrationconcentrated in vacuo
3. dissolutionThe residue was dissolved in dichloromethane
4. washwashed with water
5. concentrationconcentrated in vacuo