HRID533113

反应详情

EQUATION

反应方程式

HRID 533113 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A solution of HCl in dioxane (4 N, 5.0 mL) is added to 4-[5-(4-methanesulfonyl-phenyl)-2,3-dihydro-benzofuran-2-yl]-piperidine-1-carboxylic acid tert-butyl ester (750 mg) in dichloromethane (1 mL) and the resulting mixture is stirred for 5 min at room temperature. The solvents are evaporated in vacuo to give the title compound as its hydrochloric acid salt. Mass spectrum (ESI+): m/z=358 [M+H]+.

WORKUP

后处理

  1. customThe solvents are evaporated in vacuo