HRID535284

反应详情

EQUATION

反应方程式

HRID 535284 的结构方程式

REACTANTS

反应物

3

结构：CCN(C(C)C)C(C)C

Diisopropylethylamine

C8H19N

结构：CN(C)C(ON1C(=O)CCC1=O)=[N+](C)C.F[B-](F)(F)F

TSTU

C9H16BF4N3O3

结构：CC(C)(C)OC(=O)CCCCCCC(=O)O

未命名化合物

PRODUCTS

生成物

1

结构：CC(C)(C)OC(=O)CCCCCCC(=O)ON1C(=O)CCC1=O

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1

结构：C1CCOC1

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

Octanedioic acid mono-tert-butyl ester (3.14 g, 13.63 mmol) was dissolved in THF (100 mL). TSTU (4.9 g, 16.3 mmol) was added and pH was adjusted to 8.5 with DIPEA (2.85 mL).