Glycine → HCID 13822947, compound

HRID 543003Notes

Reaction equation

HRID 543003 reaction equation
[NH2:1][CH2:2][C:3]([OH:5])=O.ClC(OCC1C=CC=CC=1)=O.ClC(OCC)=O.[CH2:23]([NH2:30])[CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH3:29]>C(N(CC)CC)C>[CH2:23]([NH:30][C:3](=[O:5])[CH2:2][NH2:1])[CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH3:29]

Participants

6

Reactant 4

HCID 750GlycineHCID 81271-HeptanamineHCID 10387Benzyl chloroformateHCID 10928Ethyl chloroformate

Product 1

HCID 13822947HCID 13822947, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

As above from glycine and benzyl chloroformate (N-benzyloxycarbonylglycine has m.p. 119°-121° C.), then triethylamine, ethyl chloroformate and n-heptylamine.

Sources & evidence

ORD record
ord-86fd63024b744867ae27a52350b7f858
Source dataset
uspto-grants-1987_04
Patent number
US04659516

Reaction notes

Loading…