Hydrochloric Acid → HCID 12823310, compound

HRID 543765Notes

Reaction equation

HRID 543765 reaction equation
[N:1]([O-])=O.[Na+].[NH2:5][C:6]1[CH:7]=[C:8]([CH:12]=[CH:13][CH:14]=1)[C:9]([OH:11])=[O:10].[ClH:15]>O>[Cl-:15].[C:9]([C:8]1[CH:7]=[C:6]([N+:5]#[N:1])[CH:14]=[CH:13][CH:12]=1)([OH:11])=[O:10]

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 74193-Aminobenzoic AcidHCID 23668193Sodium Nitrite

Product 1

HCID 12823310HCID 12823310, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

A solution of NaNO2 (36.2 g.) in water (300 ml.) was added during approximately 30 minutes to a suspension of 3-aminobenzoic acid (68.6 g.) in concentrated hydrochloric acid (126.3 ml.) and water (200 ml.) at 0°-5°. The mixture was filtered to give a solution of 3-carboxybenzenediazonium chloride.

Workup

  1. filtrationThe mixture was filtered

Sources & evidence

ORD record
ord-558cce4671f2485fbff6fdc1ef5ff610
Source dataset
uspto-grants-1984_05
Patent number
US04447441

Reaction notes

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