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HRID544508

反应详情

EQUATION

反应方程式

HRID 544508 的结构方程式

REACTANTS

反应物

2
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：COc1cc(C(=O)CC(O)C(=O)O)cc(OC)c1OC
HCID3069179

2-Hydroxy-4-oxo-4-(3,4,5-trimethoxyphenyl)butanoic acid

C13H16O7

PRODUCTS

生成物

1
结构：COc1cc(C(=O)/C=C/C(=O)O)cc(OC)c1OC
HCID6366494

Baxitozine

C13H14O6

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(=O)O
溶剂HCID176

Acetic Acid

C2H4O2

PROCEDURE

实验过程

15.8 g of 4-(3,4,5-trimethoxyphenyl)-4-oxo-2-hydroxy butanoic acid obtainedin Example 3, 20 cc of acetic acid and 20 cc of concentrated hydrochloric acid (d-1.18) are heated for 2.5 hours under reflux.

WORKUP

后处理

  1. temperatureunder reflux