HRID55127
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
To a solution containing 3-thiophenemethanol (0.45 g, 0.0033×1.2 mol) and sodium hydride (0.14 g, (ca.60% in mineral oil), 0.033×1.05 mol) in tetrahydrofuran, 2,6- dichloro-4-methoxypyridine (0.59 g, 0.0033 mol) was added and the resultant solution was refluxed for about 2 hours.
WORKUP
后处理
- additionwas added