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HRID551508

反应详情

EQUATION

反应方程式

HRID 551508 的结构方程式

REACTANTS

反应物

3
结构：CC(C)(C)OC(=O)OC(=O)OC(C)(C)C
HCID90495

Di-tert-butyl dicarbonate

C10H18O5

结构：O=Cc1cccc2[nH]ccc12
HCID333703

Indole-4-carboxaldehyde

C9H7NO

结构：CC(C)(C)OC(=O)n1ccc2ccc(C=O)cc21
HCID14616867

1,1-Dimethylethyl 6-formyl-1H-indole-1-carboxylate

C14H15NO3

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)n1ccc2c(C=O)cccc21
HCID49758854

tert-Butyl 4-formyl-1H-indole-1-carboxylate

C14H15NO3

PROCEDURE

实验过程

4-Formyl-indole-1-carboxylic acid tert-butyl ester was synthesized by a procedure similar to 6-Formyl-indole-1-carboxylic acid tert-butyl ester from starting materials 1H-Indole-4-carbaldehyde and di-tert-butyl-dicarbonate to yield the product as a clear yellow oil (2 g, 80%). LC-MS (ES) calculated for C14H15NO3, 245.1; found m/z 244 [M−H]−.