HRID554327

反应详情

EQUATION

反应方程式

HRID 554327 的结构方程式

PROCEDURE

实验过程

By a reaction under similar conditions as in Reference Example 234 and using 5-phenyl-1H-pyrrole-3-carbaldehyde (342 mg), sodium hydride (60% in oil, 120 mg), 15-crown-5 (0.60 mL) and 2-chloro-5-pyrimidinesulfonyl chloride (554 mg), the title compound was obtained as a yellow solid (yield 390 mg, 56%).

WORKUP

后处理

  1. customBy a reaction under similar conditions as in Reference Example 234