Hydrochloric Acid → HCID 86617049, compound

HRID 555191Notes

Reaction equation

[C:1](O)(=[O:5])[CH:2]([CH3:4])[OH:3].[OH:7][CH:8]1[O:16][C@H:15]([CH2:17][OH:18])[C@@H:13]([OH:14])[C@H:11]([OH:12])[C@H:9]1[NH2:10].Cl.O=C[C@@H]([C@H]([C@@H]([C@@H](CO)O)O)O)O>>[C:1]([NH:10][C@@H:9]1[C@@H:11]([OH:12])[C@H:13]([OH:14])[C@@H:15]([CH2:17][OH:18])[O:16][CH:8]1[OH:7])(=[O:5])[CH:2]([CH3:4])[OH:3]

Participants

Reactant 4

HCID 313Hydrochloric Acid

HCID 612Lactic Acid

HCID 107526(2R,3S,4R,5R)-2,3,4,5,6-pentahydroxyhexanal

HCID 439213D-Glucosamine

Product 1

HCID 86617049HCID 86617049, compound

Procedure

75 g of lactic acid (90% pure) was mixed with 22.5 g of glucosamine.HCl and 2.5 g of Dextrose. The mixture was reacted at 120 C for 4 hours. The reacted mixture was cooled down and stored at 4 C.

Workup

customThe mixture was reacted at 120 C for 4 hours
temperatureThe reacted mixture was cooled down

Sources & evidence

ORD record: ord-880e67c3b22847379d4f01f5a37e2e9c
Source dataset: uspto-grants-2011_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08053013B2

Reaction notes

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