HRID557174

反应详情

EQUATION

反应方程式

HRID 557174 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Add 2-bromo-1,1-diethoxyethane (3.64 g, 18.48 mmol) to a solution of 6-bromopyridin-2-ylamine (1.0 g, 5.77 mmol) in n-butanol (40 ml). Reflux the reaction overnight, cool. Filtration of the reaction mixture gives 5-bromoimidazo[1,2-a]pyridine hydrobromide as a white solid.

WORKUP

后处理

  1. temperatureReflux
  2. customthe reaction overnight
  3. temperaturecool
  4. filtrationFiltration of the reaction mixture