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HRID55747

反应详情

EQUATION

反应方程式

HRID 55747 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)O
HCID6386

tert-Butyl alcohol

C4H10O

结构：O=C(Cl)C(=O)Cl
HCID65578

Ethanedioyl dichloride

C2Cl2O2

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)C(=O)Cl
HCID11126621

tert-butyl 2-chloro-2-oxoacetate

C6H9ClO3

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCOCC
溶剂HCID3283

Diethyl Ether

C4H10O

PROCEDURE

实验过程

Oxalyl chloride (232 μL, 2.8 mmol) and t-butyl alcohol (228 μL) were combined in ether (6.7 mL) under nitrogen at 0° C. The resulting mixture was stirred for 30 minutes at room temperature. The solvent was evaporated under vacuum to form Compound 34.

WORKUP

后处理

  1. customThe solvent was evaporated under vacuum