反应详情

温度

60 °C

The product from example 1 step (vii) (0.15 g) was dissolved in DMSO (2 mL) and succinimide (0.25 g) and potassium carbonate (0.07 g) was added. The reaction mixture stirred at 60° C. for 16 h. The reaction mixture was filtered through a filter disc and purified via RP-prep-HPLC to give title the compound (0.065 g)

1. filtrationThe reaction mixture was filtered through a filter disc
2. custompurified via RP-prep-HPLC