HRID566981

反应详情

EQUATION

反应方程式

HRID 566981 的结构方程式

PROCEDURE

实验过程

Following the procedure of Example B2, 2-benzyloxy-6-chloro-5-cyano-benzo[de]isoquinoline-1,3-dione (0.20 g, 0.55 mmol, from Example A2), piperidine (0.11 g, 1.1 mmol), and triethyl amine (0.11 g, 1.1 mmol) were reacted at ambient temperature for 5 hours to give 0.17 g of the title compound.

WORKUP

后处理

  1. customwere reacted at ambient temperature for 5 hours