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HRID567072

反应详情

EQUATION

反应方程式

HRID 567072 的结构方程式

REACTANTS

反应物

3
结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：CCOCCCBr
HCID260493

1-bromo-3-ethoxypropane

C5H11BrO

结构：COCCN(C1CC(C)(C)Oc2ccc(O)cc21)S(C)(=O)=O
HCID17786848

未命名化合物

PRODUCTS

生成物

1
结构：CCOCCCOc1ccc2c(c1)C(N(CCOC)S(C)(=O)=O)CC(C)(C)O2
HCID9866555

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCCCCCC.CCOC(C)=O
溶剂HCID21899848

未命名化合物

PROCEDURE

实验过程

0.5 g (1.5 mmol) of N-[2,2-dimethyl-6-hydroxychroman-4-yl]-N-(2-methoxyethyl)methanesulfonamide (Example 16b) was reacted with potassium carbonate and 3-ethoxy-1-bromopropane analogously to Example 1g. After column chromatography on silica gel using n-heptane/EA (5:1), 0.35 g of oily product was obtained.