HRID568647

反应详情

EQUATION

反应方程式

HRID 568647 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

The Friedel-Crafts procedure of Example 24a is repeated with 31.55 g of p-fluorobenzoyl chloride, 32 g of 2,3-dichloroanisole and 35.22 g of AlCl3 combined in 1,2-dichloroethane and reacted. The resultant crude product is triturated with warm hexane, cooled and filtered to yield 2,3-dichloro-4-methoxy-4'-fluorobenzophenone.

WORKUP

后处理

  1. customreacted
  2. customThe resultant crude product is triturated with warm hexane
  3. temperaturecooled
  4. filtrationfiltered