huagongshe.com
HRID575777

反应详情

EQUATION

反应方程式

HRID 575777 的结构方程式

REACTANTS

反应物

2
结构：CCOC(C)=O
HCID8857

Ethyl acetate

C4H8O2

结构：CCc1ccc(S(C)(=O)=O)cc1[N+](=O)[O-]
HCID58266121

未命名化合物

PRODUCTS

生成物

1
结构：CCc1ccc(S(C)(=O)=O)cc1N
HCID28355896

未命名化合物

收率 94.6%

AUXILIARIES

试剂、催化剂与溶剂

2
结构：[Pd]
催化剂HCID23938

Palladium

Pd

结构：CO
溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

The title compound of step 1 (0.6 g, 2.6 mmol) and palladium on carbon (0.18 g) in CH3OH (20 mL) was hydrogenated at 1 atm. for 6 h. Silica gel chromatography (PE:EA=6:1) gave the title compound (0.49 g, 94%) as a brown liquid.