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HRID580512

反应详情

EQUATION

反应方程式

HRID 580512 的结构方程式

REACTANTS

反应物

3
结构：CC(=O)C[N+](=O)[O-]
HCID66296

2-Propanone, 1-nitro-

C3H5NO3

结构：O=Cc1ccccc1-c1ccccc1C(F)(F)F
HCID1392725

未命名化合物

结构：C/C(N)=C/C(=O)N1CCN(C2CCCCC2)CC1
HCID86742239

未命名化合物

PRODUCTS

生成物

1
结构：CC1=C(C(=O)N2CCN(C3CCCCC3)CC2)C(c2ccccc2C(F)(F)F)C([N+](=O)[O-])=C(C)N1
HCID86742240

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC(C)O
溶剂HCID3776

Isopropanol

C3H8O

PROCEDURE

实验过程

17.4 g (0.10 mol) of 2-trifluoromethylphenylbenzaldehyde, 12.0 g (0.12 mol) of nitroacetone and 25.1 g (0.10 mol) of β-aminocrotonic acid 4-cyclohexylpiperazide are heated in 50 ml of isopropanol at 60° C. for 12 hours. On cooling, the product separates out and is recrystallized from isopropanol.

WORKUP

后处理

  1. temperatureOn cooling
  2. customis recrystallized from isopropanol