HRID581185

反应详情

EQUATION

反应方程式

HRID 581185 的结构方程式

PROCEDURE

实验过程

Reaction was performed by using the following reactants, catalyst and solvent: 1-amino-4-anilinoanthraquinone (precursor, 2.5 g, 7.96 mmol), 4-vinylbenzyl chloride (1.25 g, 8.22 mmol), 2,6-lutidine (a catalyst, 0.88 g, 8.22 mmol) and acetonitrile (solvent, 25 ml) in a reaction apparatus similar to that of Example 1. After completion of the reaction, the product was purified in the same manner as in Example 1 to afford the desired reactive dye, BD-4 (Yield: 67%). ##STR9##

WORKUP

后处理

  1. customReaction
  2. customAfter completion of the reaction
  3. customthe product was purified in the same manner as in Example 1
  4. customto afford the desired reactive dye, BD-4 (Yield: 67%)