HRID581841

反应详情

EQUATION

反应方程式

HRID 581841 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

The preparation is carried out analogously to Examples XLIIa to c. Instead of ethyl bromoacetate, cyclohexyl bromoacetate (boiling point: 102-104° C. under 16 mbar, prepared by reaction of bromoacetyl chloride with cyclohexanol in pyridine/ethyl acetate in the presence of a catalytic amount of 4-dimethylaminopyridine) is employed. Melting point: 85-88° C.