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HRID584326

反应详情

EQUATION

反应方程式

HRID 584326 的结构方程式

REACTANTS

反应物

1
结构：CCC(=O)c1ccc(-c2cc(NCc3ccc(COC(=O)c4ccccc4)c(COC(=O)c4ccccc4)c3)ccc2C)c(C)c1
HCID69792603

未命名化合物

PRODUCTS

生成物

1
结构：CCC(=O)c1ccc(-c2cc(NCc3ccc(CO)c(CO)c3)ccc2C)c(C)c1
HCID22345635

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O=C([O-])[O-].[K+].[K+]
溶剂HCID11430

Potassium Carbonate

CK2O3

PROCEDURE

实验过程

800 mg (1.3 mmol) of 2-benzoyloxymethyl-5-[(6,2′-dimethyl-4′-propionylbiphenyl-3-ylamino)methyl]benzyl benzoate are dissolved in methanolic 2% potassium carbonate solution and the medium is stirred for 1 hour. After water/dichloromethane extraction, the residue obtained is purified by chromatography on silica gel (eluent: 30 heptane/70 ethyl acetate). A yellow oil is obtained (m=470 mg, Y=88%).

WORKUP

后处理

  1. extractionAfter water/dichloromethane extraction
  2. customthe residue obtained
  3. customis purified by chromatography on silica gel (eluent: 30 heptane/70 ethyl acetate)
  4. customA yellow oil is obtained (m=470 mg, Y=88%)