HRID585484

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID75818

L-alpha-Methylbenzylamine

C8H11N

结构：CCOc1ccc(C(=O)[C@H]2CC=CC[C@H]2C(=O)O)cc1OCC

HCID10925192

未命名化合物

2 次

HCID22311317

4-Hydrazinylpiperidine--hydrogen chloride (1/2)

C5H15Cl2N3

PRODUCTS

生成物

结构：CCOc1ccc(C2=NN(C3CCNCC3)C(=O)[C@@H]3CC=CC[C@H]23)cc1OCC.Cl

HCID68877453

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID3776

Isopropanol

C3H8O

PROCEDURE

实验过程

Prepared from the salt of (S)-(−)-α-methylbenzylamine, (cis)-2-(3,4-diethoxybenzoyl)-1,2,3,6-tetrahydrobenzoic acid (compound P) and piperidin-4-yl-hydrazine dihydrochloride in 2-propanol as described for compound 5d. M. p. 248-250° C.