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HRID585740

反应详情

EQUATION

反应方程式

HRID 585740 的结构方程式

REACTANTS

反应物

2
结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：COC(=O)c1ccc2c(c1)SCC[C@@H]2NC(=O)OC(C)(C)C
HCID59089451

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)N[C@H]1CCSc2cc(C(=O)O)ccc21
HCID59089455

未命名化合物

收率 96.2%

PROCEDURE

实验过程

By a similar reaction operation as in Starting Material Synthetic Example 6 using (S)-4-(tert-butoxycarbonylamino)thiochromane-7-carboxylic acid methyl ester (5.75 g) and potassium carbonate (4.91 g), the objective (S)-4-(tert-butoxycarbonylamino)thiochromane-7-carboxylic acid (5.29 g) was obtained as colorless crystals.