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HRID585751

反应详情

EQUATION

反应方程式

HRID 585751 的结构方程式

REACTANTS

反应物

2
结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：COC(=O)c1cc2c(cc1C)[C@@H](NC(=O)OC(C)(C)C)CCS2
HCID59089450

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cc2c(cc1C(=O)O)SCC[C@@H]2NC(=O)OC(C)(C)C
HCID59089485

未命名化合物

收率 77.9%

PROCEDURE

实验过程

By a similar reaction operation as in Starting Material Synthetic Example 6 using (S)-4-(tert-butoxycarbonylamino)-6-methylthiochromane-7-carboxylic acid methyl ester (8.10 g) and potassium carbonate (9.94 g), the objective (S)-4-(tert-butoxycarbonylamino)-6-methylthiochromane-7-carboxylic acid (6.05 g) was obtained as colorless crystals.