Acetaldehyde → HCID 86586498, compound

HRID 586579Notes

Reaction equation

HRID 586579 reaction equation
[NH2:1][C:2]1[S:3][CH:4]=[CH:5][N:6]=1.[N+:7]([CH2:9][C:10]([O:12][CH3:13])=[O:11])#[C-:8].[CH:14](=O)[CH3:15]>Cl(O)(=O)(=O)=O>[CH3:14][C:15]1[N:1]=[C:2]2[N:6]([C:8]=1[NH:7][CH2:9][C:10]([O:12][CH3:13])=[O:11])[CH:5]=[CH:4][S:3]2

Participants

5

Reactant 3

HCID 177AcetaldehydeHCID 21552-AminothiazoleHCID 547815Methyl isocyanoacetate

Product 1

HCID 86586498HCID 86586498, compound

Reagents, catalysts & solvents 1

HCID 24247Perchloric AcidSolvent

Procedure

Compound 23 was prepared in accordance with the general synthesis instructions from 1.0 ml (0.1 mmol) 2-aminothiazole solution (0.1 M, MC), 0.575 ml (0.115 mmol) methyl isocyanoacetate solution (0.2 M, MC), 0.500 ml (0.15 mmol) acetaldehyde solution (0.3 M, MC) and 10 μl perchloric acid (w=20%) in a substance library.

Sources & evidence

ORD record
ord-5d0f6fd7e598468ca8d8fc5a74246b5e
Source dataset
uspto-grants-2005_08
Patent number
US06936631B2

Reaction notes

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