HRID589758

反应详情

EQUATION

反应方程式

HRID 589758 的结构方程式

PROCEDURE

实验过程

The product was prepared according to General Procedure 6, described in Example 65, with 5-methylbenzothiophene-2-sulfonyl chloride (30.0 mg, 0.12 mmol), pyridine (49 μL, 0.61 mmol) and 3-aminobenzoic acid (16.7 mg, 0.10 mmol). The title compound was obtained in 66% yield (23 mg). MS (ESI+) calcd mass for C16H13NO4S2 347.028599, found 347.029559.

WORKUP

后处理

  1. customThe product was prepared