HRID59086

反应详情

EQUATION

反应方程式

HRID 59086 的结构方程式

PROCEDURE

实验过程

To a solution of 2,4-dichloro-6-((2,2,2-trifluoroethoxy)methyl)pyrimidine (200 mg, 0.77 mmol) in acetonitrile (3 mL) was benzylmethylamine (0.296 mL, 2.30 mmol) added. The reaction was stirred at ambient temperature for 30 minutes. The solvent was evaporated. The mixture was purified by preparative HPLC the title compound (194 mg, 73%).

WORKUP

后处理

  1. additionadded
  2. customThe solvent was evaporated
  3. customThe mixture was purified by preparative HPLC the title compound (194 mg, 73%)