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HRID594626

反应详情

EQUATION

反应方程式

HRID 594626 的结构方程式

REACTANTS

反应物

2
结构：BrCC1CC1
HCID81503

Bromomethylcyclopropane

C4H7Br

结构：COc1cccc(OC)c1C1CCCC(=O)N1Cc1ccc(O)cc1
HCID69081744

未命名化合物

PRODUCTS

生成物

1
结构：COc1cccc(OC)c1C1CCCC(=O)N1Cc1ccc(OCC2CC2)cc1
HCID69084592

未命名化合物

PROCEDURE

实验过程

Prepared according to the described general procedure 7 (GP7) by O-alkylation of 6-(2,6-dimethoxyphenyl)-1-(4-hydroxybenzyl)piperidin-2-one with commercially available (bromomethyl)cyclopropane. Subsequent purification by preparative HPLC afforded the target compound. LC-MS (conditions E): tR=0.78 min.; [M+H]+: 396.27 g/mol.

WORKUP

后处理

  1. customPrepared
  2. customSubsequent purification by preparative HPLC
  3. customafforded the target compound