2-Bromopropane → HCID 70638305, compound

HRID 597144Notes

Reaction equation

HRID 597144 reaction equation
[CH3:1][N:2]([CH2:4][C:5]([C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][C:16]=1[O:21][CH3:22])=[CH:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[O:13][CH3:14])[CH3:3].[CH:23]([Br:26])([CH3:25])[CH3:24]>C(OCC)(=O)C>[Br-:26].[CH:23]([N+:2]([CH2:4][C:5]([C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][C:16]=1[O:21][CH3:22])=[CH:6][C:7]1[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=1[O:13][CH3:14])([CH3:1])[CH3:3])([CH3:25])[CH3:24]

Participants

4

Reactant 2

HCID 63582-BromopropaneHCID 54558058HCID 54558058, compound

Product 1

HCID 70638305HCID 70638305, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

2.2 Parts of N,N-dimethyl-2,3-di(2-methoxyphenyl)allylamine is combined with 5 parts by volume of isopropyl bromide. That mixture is allowed to stand at 65° for 21 days. Ethyl acetate is added to the solid which forms and the solid is broken and triturated. That mixture then is filtered, and the solid collected is washed with ethyl acetate and dried to afford N-isopropyl-N,N-dimethyl-2,3-di(2-methoxyphenyl)allylammonium bromide. That compound is structurally represented by the following formula ##STR10##

Workup

  1. customtriturated
  2. filtrationThat mixture then is filtered
  3. customthe solid collected
  4. washis washed with ethyl acetate
  5. customdried

Sources & evidence

ORD record
ord-3c0baaa5d78643728459070cfdda945a
Source dataset
uspto-grants-1977_03
Patent number
US04013643

Reaction notes

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