Diethylamine → HCID 70632819, compound

HRID 597166Notes

Reaction equation

HRID 597166 reaction equation
[O:1]([CH2:8][C:9]([NH:11][CH:12]1[C:37](=[O:38])[N:14]2[C:15]([C:25]([O:27][CH2:28][C:29]3[CH:34]=[CH:33][C:32]([O:35][CH3:36])=[CH:31][CH:30]=3)=[O:26])=[C:16](OS(CC)(=O)=O)[CH2:17][S:18][C@H:13]12)=[O:10])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH2:39]([NH:41][CH2:42][CH3:43])[CH3:40]>C1COCC1>[O:1]([CH2:8][C:9]([NH:11][CH:12]1[C:37](=[O:38])[N:14]2[C:15]([C:25]([O:27][CH2:28][C:29]3[CH:34]=[CH:33][C:32]([O:35][CH3:36])=[CH:31][CH:30]=3)=[O:26])=[C:16]([N:41]([CH2:42][CH3:43])[CH2:39][CH3:40])[CH2:17][S:18][C@H:13]12)=[O:10])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

4

Reactant 2

HCID 8021DiethylamineHCID 88815802HCID 88815802, compound

Product 1

HCID 70632819HCID 70632819, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

p-Methoxybenzyl 7-phenoxyacetamido-3-diethylamino-3-cephem-4-carboxylate is prepared with p-methoxybenzyl 7-phenoxyacetamido-3-ethylsulfonyloxy-3-cephem-4-carboxylate and diethylamine in THF.

Sources & evidence

ORD record
ord-f2aaf7fdde734cb2ad8f4dade6a4f9a2
Source dataset
uspto-grants-1977_03
Patent number
US04013651

Reaction notes

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