Hydrochloric Acid → HCID 131710697, compound

HRID 597235Notes

Reaction equation

HRID 597235 reaction equation
[ClH:1].[CH2:2]([N:4]1[N:15]=[CH:14][C:13]2[C:12]3[N:11]([CH3:16])[N:10]=[C:9]4[C:17]5[CH:24]=[CH:23][CH:22]=[CH:21][C:18]=5[CH2:19][CH2:20][C:7]([C:8]=34)=[N:6][C:5]1=2)[CH3:3]>C(OCC)(=O)C>[ClH:1].[CH2:2]([N:4]1[N:15]=[CH:14][C:13]2[C:12]3[N:11]([CH3:16])[N:10]=[C:9]4[C:17]5[CH:24]=[CH:23][CH:22]=[CH:21][C:18]=5[CH2:19][CH2:20][C:7]([C:8]=34)=[N:6][C:5]1=2)[CH3:3]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 21447177HCID 21447177, compound

Product 1

HCID 131710697HCID 131710697, compoundYield 92%

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

Addition of ethereal hydrochloric acid to a solution of 5-ethyl-2,5,7,8-tetrahydro-2-methyl-1,2,4,5,6-pentaazabenzo[6,7]cyclohepta[1,2,3-cd]-as-indacene in ethyl acetate provides the hydrochloride, yield 92%, m.p. 208°-211° (dec.).

Sources & evidence

ORD record
ord-734912aa209847d88b9b3d976a3b2279
Source dataset
uspto-grants-1977_03
Patent number
US04013672

Reaction notes

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