HRID600615

反应详情

EQUATION

反应方程式

HRID 600615 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

120 mg of (6-methylimidazo[1,2-a]pyridin-2-yl)phenylmethanone are taken up in 2 mL of ethanol and the solution is treated with 1.5 mL of a 4N solution of hydrogen chloride in dioxane and then with 2 mL of diethyl ether. The crystals obtained are filtered off and washed with diethyl ether, and then dried. 77 mg of (6-methylimidazo[1,2-a]pyridin-2-yl)phenylmethanone hydrochloride (1:1) are obtained in the form of a beige-colored solid.

WORKUP

后处理

  1. customThe crystals obtained
  2. filtrationare filtered off
  3. washwashed with diethyl ether
  4. customdried