Benzyl Bromide → HCID 86592118, compound

HRID 601144Notes

Reaction equation

HRID 601144 reaction equation
[NH:1]1[C:6]2N=[CH:8][CH:9]=[CH:10][C:5]=2[C:4](=[O:11])[O:3][C:2]1=[O:12].[CH2:13](Br)[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1.[CH2:21](Br)CCC>>[CH2:13]([N:1]1[C:6]2[CH2:21][CH2:8][CH2:9][CH2:10][C:5]=2[C:4](=[O:11])[O:3][C:2]1=[O:12])[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1

Participants

4

Reactant 3

HCID 7498Benzyl BromideHCID 8002Butyl bromideHCID 109865823-Azaisatoic anhydride

Product 1

HCID 86592118HCID 86592118, compound

Procedure

The title compound was prepared according to the procedure of Example 1B substituting the product of Example 113A for the product of Example 1A and substituting benzyl bromide for n-butyl bromide (0.620 g, 67%). MS (ESI−) m/z 256 (M−H)−.

Sources & evidence

ORD record
ord-d5deaa6754f74a2a827449003947ca35
Source dataset
uspto-grants-2011_03
Patent number
US07902203B2

Reaction notes

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