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HRID602628

反应详情

EQUATION

反应方程式

HRID 602628 的结构方程式

REACTANTS

反应物

3
结构：ClCCCBr
HCID8006

1-Bromo-3-chloropropane

C3H6BrCl

结构：O=C([O-])[O-].[Cs+].[Cs+]
HCID10796

Cesium carbonate

CCs2O3

结构：NC(=O)c1ccc(O)cc1
HCID65052

4-Hydroxybenzamide

C7H7NO2

PRODUCTS

生成物

1
结构：NC(=O)c1ccc(OCCCCl)cc1
HCID14407176

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CC#N
溶剂HCID6342

Acetonitrile

C2H3N

PROCEDURE

实验过程

A mixture composed of 0.004 mole of 4-hydroxybenzamide, 0.004 mole of 1-bromo-3-chloropropane and 0.006 mole of caesium carbonate in 10 ml of acetonitrile is heated at reflux for 5 hours.

WORKUP

后处理

  1. temperatureis heated
  2. temperatureat reflux for 5 hours