反应详情

tert-Butyl ((3-methylpyridin-2-yl)methyl)carbamate (4.5 g) and benzyl bromide (2 eq) in 80 ml of acetonitrile was heated in a sealed tube at reflux overnight and then concentrated in vacuo to give the title compound and was used without further purification. MS (ESI) 313 (M+H)

1. temperatureat reflux overnight
2. concentrationconcentrated in vacuo