HRID611113

反应详情

EQUATION

反应方程式

HRID 611113 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

N,N-Dimethyl-[5-(3-benzoylbenzoyl)-4,5,6,7-tetrahydrofuro[3,2-c]pyridin-2-ylmethyl]amine 0.155 g was dissolved in 2 ml of methanol; hydrogen chloride in ethyl acetate was added in excess, followed by stirring. After this mixture was concentrated, the resulting foam was washed with diethyl ether to yield the desired product.

WORKUP

后处理

  1. concentrationAfter this mixture was concentrated
  2. washthe resulting foam was washed with diethyl ether