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HRID611127

反应详情

EQUATION

反应方程式

HRID 611127 的结构方程式

REACTANTS

反应物

2
结构：Cl
HCID313

Hydrochloric Acid

ClH

结构：CN(C)Cc1cc2c(o1)CN(C(=O)c1ccc(-c3ccccc3)cc1)CC2
HCID19600119

未命名化合物

PRODUCTS

生成物

1
结构：CN(C)Cc1cc2c(o1)CN(C(=O)c1ccc(-c3ccccc3)cc1)CC2.Cl
HCID19600118

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：CO
溶剂HCID887

Methanol

CH4O

结构：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

N,N-Dimethyl-[6-(4-phenylbenzoyl)-4,5,6,7-tetrahydrofuro[2,3-c]pyridin-2-ylmethyl]amine 0.180 g was dissolved in 2 ml of methanol; hydrogen chloride in ethyl acetate was added in excess, followed by stirring. After concentration, the crude product recrystallized from ethanol-diethyl ether to yield the desired product.

WORKUP

后处理

  1. concentrationAfter concentration
  2. customthe crude product recrystallized from ethanol-diethyl ether