Hydrochloric Acid → HCID 67696402, compound

HRID 611144Notes

Reaction equation

HRID 611144 reaction equation
[CH3:1][N:2]([CH2:4][C:5]1[O:32][C:8]2[CH2:9][N:10]([C:13]([C:15]3[CH:16]=[CH:17][C:18]4[C:19](=[O:31])[C:20]5[C:25]([S:26](=[O:30])(=[O:29])[C:27]=4[CH:28]=3)=[CH:24][CH:23]=[CH:22][CH:21]=5)=[O:14])[CH2:11][CH2:12][C:7]=2[CH:6]=1)[CH3:3].[ClH:33]>CO.C(OCC)(=O)C>[ClH:33].[CH3:3][N:2]([CH2:4][C:5]1[O:32][C:8]2[CH2:9][N:10]([C:13]([C:15]3[CH:16]=[CH:17][C:18]4[C:19](=[O:31])[C:20]5[C:25]([S:26](=[O:30])(=[O:29])[C:27]=4[CH:28]=3)=[CH:24][CH:23]=[CH:22][CH:21]=5)=[O:14])[CH2:11][CH2:12][C:7]=2[CH:6]=1)[CH3:1]

Participants

5

Reactant 2

HCID 313Hydrochloric AcidHCID 67696209HCID 67696209, compound

Product 1

HCID 67696402HCID 67696402, compound

Reagents, catalysts & solvents 2

HCID 887MethanolSolventHCID 8857Ethyl AcetateSolvent

Procedure

N,N-Dimethyl-[6-(9,10,10-trioxo-9,10-dihydro-10λ6 -thioxanthene-3-carbonyl)-4,5,6,7-tetrahydrofuro[2,3-c]pyridin-2-ylmethyl]amine 0.133 g was dissolved in 2 ml of methanol; hydrogen chloride in ethyl acetate was added in excess, followed by stirring. After this mixture was concentrated, the resulting solid was washed with diethyl ether to yield the desired product.

Workup

  1. concentrationAfter this mixture was concentrated
  2. washthe resulting solid was washed with diethyl ether

Sources & evidence

ORD record
ord-240b9dc3a77448c09e8ba92104a1d2f7
Source dataset
uspto-grants-1999_12
Patent number
US05998433

Reaction notes

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