Hydrochloric Acid → HCID 67698164, compound

HRID 611147Notes

Reaction equation

HRID 611147 reaction equation
[CH3:1][N:2]([CH2:4][C:5]1[O:13][C:12]2[CH2:11][CH2:10][N:9]([C:14]([C:16]3[CH:17]=[CH:18][C:19]4[C:20](=[O:32])[C:21]5[C:26]([S:27](=[O:31])(=[O:30])[C:28]=4[CH:29]=3)=[CH:25][CH:24]=[CH:23][CH:22]=5)=[O:15])[CH2:8][C:7]=2[CH:6]=1)[CH3:3].[ClH:33]>CO.C(OCC)(=O)C>[ClH:33].[CH3:3][N:2]([CH2:4][C:5]1[O:13][C:12]2[CH2:11][CH2:10][N:9]([C:14]([C:16]3[CH:17]=[CH:18][C:19]4[C:20](=[O:32])[C:21]5[C:26]([S:27](=[O:30])(=[O:31])[C:28]=4[CH:29]=3)=[CH:25][CH:24]=[CH:23][CH:22]=5)=[O:15])[CH2:8][C:7]=2[CH:6]=1)[CH3:1]

Participants

5

Reactant 2

HCID 313Hydrochloric AcidHCID 67698165HCID 67698165, compound

Product 1

HCID 67698164HCID 67698164, compound

Reagents, catalysts & solvents 2

HCID 887MethanolSolventHCID 8857Ethyl AcetateSolvent

Procedure

N,N-Dimethyl-[5-(9,10,10-trioxo-9,10-dihydro-10λ6 -thioxanthene-3-carbonyl)-4,5,6,7-tetrahydrofuro[3,2-c]pyridin-2-ylmethyl]amine 0.088 g was dissolved in 2 ml of methanol; hydrogen chloride in ethyl acetate was added in excess, followed by stirring. After this mixture was concentrated, the resulting solid was washed with diethyl ether to yield the desired product.

Workup

  1. concentrationAfter this mixture was concentrated
  2. washthe resulting solid was washed with diethyl ether

Sources & evidence

ORD record
ord-4d0926d7ab834562952af278941934ca
Source dataset
uspto-grants-1999_12
Patent number
US05998433

Reaction notes

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