反应详情

温度

5 °C

A suspension of AD-Mix-B® (1.40 9) in water (5 ml) and t-butanol (5 ml) was cooled to 5° C. and N-(5-vinyl-pyridin-2-yl)-2,2-dimethylpropionamide (0.204 g, 1.0 mmol) was added. The mixture was stirred at 5° C. for 18 hours. The reaction mixture was then treated with sodium sulfite (3.0 g), stirred for 30 minutes and then extracted with dichloromethane.

1. stirringstirred for 30 minutes
2. extractionextracted with dichloromethane