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HRID612263

反应详情

EQUATION

反应方程式

HRID 612263 的结构方程式

REACTANTS

反应物

2
结构：O.O.[Cl][Sn][Cl]
HCID61436

Stannous chloride dihydrate

Cl2H4O2Sn

结构：N#Cc1cnc2ccc([N+](=O)[O-])cc2c1Nc1ccc(Br)c(Br)c1
HCID10114652

未命名化合物

PRODUCTS

生成物

1
结构：N#Cc1cnc2ccc(N)cc2c1Nc1ccc(Br)c(Br)c1
HCID10158966

未命名化合物

收率 27.3%

PROCEDURE

实验过程

Prepared from 4.90 g of 4-(3,4-dibromophenylamino)-6-nitroquinoline-3-carbonitrile and 12.4 g of SnCl2.2H2O in the same manner as Example 378. There was obtained 1.25 g of 6-amino-4-(3,4-dibromophenylamino)quinoline-3-carbonitrile as a brown solid: mass spectrum (electrospray, m/e): M+H 416.9, 418.9.