Ammonium Hydroxide → HCID 18779061, compound

HRID 613751Notes

Reaction equation

HRID 613751 reaction equation
[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][CH2:9][O:10][CH2:11][C:12]([OH:14])=O)=[CH:4][CH:3]=1.C(Cl)(=O)C(Cl)=O.[OH-].[NH4+:22]>C1(C)C=CC=CC=1>[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][CH2:9][O:10][CH2:11][C:12]([NH2:22])=[O:14])=[CH:4][CH:3]=1

Participants

5

Reactant 3

HCID 14923Ammonium HydroxideHCID 65578Oxalyl chlorideHCID 132089242-(4-Methylphenyl)ethoxyacetic acid

Product 1

HCID 18779061HCID 18779061, compound

Reagents, catalysts & solvents 1

HCID 1140TolueneSolvent

Procedure

The subtitle compound (0.77 g) was prepared according to the procedure in example 1 part b using 2-[2-(4-methylphenyl)ethoxy]acetic acid (1.1 g). oxalyl chloride (1.44 g), concentrated ammonium hydroxide (20 ml), and toluene (40 ml).

Sources & evidence

ORD record
ord-ca846dd7563d444cbe5a5bf235b63273
Source dataset
uspto-grants-1999_12
Patent number
US06008365

Reaction notes

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