HRID615063

反应详情

EQUATION

反应方程式

HRID 615063 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To a mixture of 3.6 g. of glyceraldehyde and 2.44 g. of 4-dimethylaminopyridine in an ice-bath is added 4.16 g. of 4-(n-hexadecylamino)benzoyl chloride hydrochloride. After 4 hours at room temperature, chloroform and water are added. The chloroform extract is chromatographed quickly and evaporated in vacuo to yield 4-(n-hexadecylamino)benzoyl glyceraldehyde.

WORKUP

后处理

  1. additionTo a mixture of 3.6 g
  2. extractionThe chloroform extract
  3. customis chromatographed quickly
  4. customevaporated in vacuo