HRID615104

反应详情

EQUATION

反应方程式

HRID 615104 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

Isostearoyl chloride, prepared from 20 g isostearic acid, 10.1 g thionyl chloride and 0.2 ml dimethyl formamide, according to the procedure of Example 1, is added to 11 g (0.09 mole) n-octylamine and 10 g. (0.10 mole) triethylamine in 100 ml ether. The reaction mixture is treated in accordance with the procedure of Example 2, yielding 22 g of an amber oil which exhibits infrared spectra values typical of a secondary amide.

WORKUP

后处理

  1. additionThe reaction mixture is treated in accordance with the procedure of Example 2