Hydrochloric Acid → HCID 131714093, compound

HRID 615132Notes

Reaction equation

HRID 615132 reaction equation
[NH2:1][C:2]1[S:3][CH:4]=[C:5]([CH2:7][C:8]([NH:10][C@@H:11]2[C:42](=[O:43])[N:13]3[C:14]([C:30]([O:32][CH:33]([O:35][C:36](=[O:41])[C:37]([CH3:40])([CH3:39])[CH3:38])[CH3:34])=[O:31])=[C:15]([CH2:18][S:19][C:20]4[N:24]([CH2:25][CH2:26][N:27]([CH3:29])[CH3:28])[N:23]=[N:22][N:21]=4)[CH2:16][S:17][C@H:12]23)=[O:9])[N:6]=1.[ClH:44]>C(OC(=O)C)C>[ClH:44].[ClH:44].[NH2:1][C:2]1[S:3][CH:4]=[C:5]([CH2:7][C:8]([NH:10][C@@H:11]2[C:42](=[O:43])[N:13]3[C:14]([C:30]([O:32][CH:33]([O:35][C:36](=[O:41])[C:37]([CH3:38])([CH3:40])[CH3:39])[CH3:34])=[O:31])=[C:15]([CH2:18][S:19][C:20]4[N:24]([CH2:25][CH2:26][N:27]([CH3:29])[CH3:28])[N:23]=[N:22][N:21]=4)[CH2:16][S:17][C@H:12]23)=[O:9])[N:6]=1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 88697063HCID 88697063, compound

Product 1

HCID 131714093HCID 131714093, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

In 25 ml of ethylacetate, 0.5 g of the compound prepared in Example 1 was dissolved and etheral hydrogen chloride was added to the solution. The precipitated powdery product was collected by filtration, washed with ether and dried to give 0.35 g of the captioned compound.

Workup

  1. filtrationThe precipitated powdery product was collected by filtration
  2. washwashed with ether
  3. customdried

Sources & evidence

ORD record
ord-55c92c40f4e4445292238560fd9416c3
Source dataset
uspto-grants-1985_02
Patent number
US04497809

Reaction notes

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